A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl–KCl molten salt

Ling Xu Yang; Ying Wang; Hai Liang Zhang; Hui Jun Liu; Chao Liu Zeng

doi:10.1080/21663831.2019.1613695

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A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl–KCl molten salt

Original Report | 更新时间：2026-08-19

- A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl–KCl molten salt
- Materials Research Letters Vol. 7, Issue 9, Pages: 361-367(2019)
- 作者机构：
  
  1. Laboratory for Corrosion and Protection Institute of Metal Research Chinese Academy of Sciences Shenyang People’s Republic of China
  2. School of Materials Science and Engineering University of Science and Technology of China
  3. Laboratory for Corrosion and Protection Institute of Metal Research Chinese Academy of Sciences
- 作者简介：
- 基金信息：
- DOI：10.1080/21663831.2019.1613695
  CLC：
- Online First：08 May 2019，
  
  Published：2019
- 稿件说明：
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Ling Xu Yang, Ying Wang, Hai Liang Zhang, et al. A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl–KCl molten salt[J]. Materials Research Letters, 2019, 7(9): 361-367.
DOI：

Ling Xu Yang, Ying Wang, Hai Liang Zhang, et al. A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl–KCl molten salt[J]. Materials Research Letters, 2019, 7(9): 361-367. DOI： 10.1080/21663831.2019.1613695.

摘要

Abstract

BSTRACTHerein we report

a simple novel method to synthesize nanosized Ti

AlC

powder from Ti

and C powders in NaCl–KCl molten salt. It is more conducive to the formation of Ti

AlC

at higher salt/precursor materials ratio and particle size of Ti

AlC

powder dramatically decreases with increasing mass ratio of the salt to precursor materials. Fine-grained Ti

AlC

powder is successfully synthesized at 950

○

C for 5 h or at 1000

○

C for 2 h with a salt/precursor materials ratio of 10:1. Ti

MXene is also prepared by etching fine-grained Ti

AlC

precursor in HF solution at 60°C for 2 h.

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Related Institution

School of Materials Engineering Purdue University West Lafayette

a School of Materials Engineering Shanxi College of Technology

b School of Materials Science and Engineering Taiyuan University of Science and Technology

c State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong University

d School of Energy and Power Engineering North University of China

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