LI Chunwei, TIAN Xiubo, JIANG Xuesong, et al. Modulation of external magnetic field on (EMF) HiPIMS discharge,deposition, and properties of vanadium films[J]. 2021, 53(8): 144-152.
DOI:
LI Chunwei, TIAN Xiubo, JIANG Xuesong, et al. Modulation of external magnetic field on (EMF) HiPIMS discharge,deposition, and properties of vanadium films[J]. 2021, 53(8): 144-152.DOI: 10.11918/202003093.
Modulation of external magnetic field on (EMF) HiPIMS discharge,deposition, and properties of vanadium films
The optimal external magnetic field parameters for stable discharge of a novel HiPIMS and obtaining high-quality film were explored
and the modulation of the external magnetic field on the discharge and deposition characteristics of electro-magnetic fields synergistically enhancing high power impulse magnetron sputtering ((E-MF) HiPIMS) was studied. The effects of coil current of external magnetic field on the discharge of HiPIMS vanadium target as well as the microstructure and properties of vanadium films were investigated. The discharge behavior of HiPIMS was monitored
and the influences of external magnetic field on the phase structure
surface morphology
cross-section morphology
friction and wear resistance
and corrosion resistance of vanadium films were studied by XRD
SEM
AFM
friction and wear tester
and electrochemical corrosion method. Results show that with the increase of the coil current
the substrate ion current increased gradually. When the coil current was 6 A
the maximum substrate ion current density reached 209.2 mA/cm2. The phase structure of vanadium film was only V (111)
but the intensity of its diffraction peak increased with the increase of coil current. The surface of vanadium film exhibited typical round-pit shape. The surface roughness decreased first and then increased
and the minimum was only 10 nm. At low coil current (<4 A)
the vanadium film showed a compact and fine crystal growth structure. With the increase of coil current
the deposition rate of the film increased gradually. When the coil current was 4 A
the friction coefficient of the vanadium film was the smallest
the wear resistance was the best
and the vanadium film samples had the best corrosion resistance.