DUDekun, YUHongfa, WUChengyou. Study on Preparation of Potassium Magnesium Phosphate Bone Cement with Lithium Magnesium Slag from Salt Lake[J]. 2023, 28(3): 98-106.
DOI:
DUDekun, YUHongfa, WUChengyou. Study on Preparation of Potassium Magnesium Phosphate Bone Cement with Lithium Magnesium Slag from Salt Lake[J]. 2023, 28(3): 98-106.DOI: 10.15938/j.jhust.2023.03.012.
Study on Preparation of Potassium Magnesium Phosphate Bone Cement with Lithium Magnesium Slag from Salt Lake
MKPC) for bone bonding was prepared by lithium halide extraction by-product from Qinghai Salt Lake with potassium dihydrogen phosphate ( KH2 PO4 ). The fitting ratios of M / P ( magnesium phosphorus ratio) 1. 5
W/ C ( water ash ratio) 0. 18 were used. The coagulation hardening properties
hydration temperature rise
composition of hydration products
and microstructure morphologies of MKPC were investigated by using X-ray diffractometer ( XRD)
scanning electron microscope ( SEM )
isothermal calorimeter
and strength testing machine
as well as the following testing equipment. The development of compressive strength and fracture resistance of MKPC in simulated body fluid was explored. The results showed that mkpc bone cement prepared by using lithium magnesium slag extracted from salt lake had a significantly longer setting hardening time
and the final setting time reached more than 30 min. The early strong characteristics were obvious and the strengthdeveloped rapidly
up to 33. 5 MPa compressive strength at 3 h and 107. 7 MPa at 28 d in natural environment
through linear fitting ofthe strength data yielded the strength growth relationship between MKPC bone cement in natural environment and simulated body fluid environment. Compressive and fracture resistance strength of MKPC bone cement in simulated physiological body fluid is about 68. 1% to 71. 1% in natural environment
satisfying the strength requirement. When 1. 5% glucose was incorporated
it was able to reduce the thermal insulation temperature rise of benchmark mkpc bone cement from 64. 7 to 42. 0℃
avoiding damage to bone tissue and meeting the requirements of bone cement standard for exothermic temperature not exceeding 50℃.