Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study

Xin Li Phuah; Jie Jian; Han Wang; Xuejing Wang; Xinghang Zhang; Haiyan Wang

doi:10.1080/21663831.2021.1927878

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Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study

Original Report | 更新时间：2026-08-19

- Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study
- Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study
- 材料研究快报（英文） 2021年9卷第9期页码：373-381
- 作者机构：
  
  1. a School of Materials Engineering Purdue University West Lafayette
  2. a School of Materials Engineering Purdue University West Lafayette IN USA
  3. b School of Electrical and Computer Engineering Purdue University West Lafayette
- 作者简介：
- 基金信息：
- DOI：10.1080/21663831.2021.1927878
  中图分类号：
- 网络首发：2021-05-21，
  
  纸质出版：2021
- 稿件说明：
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Xin Li Phuah, Jie Jian, Han Wang, 等. Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study[J]. 材料研究快报（英文）, 2021,9(9):373-381.

Xin Li Phuah, Jie Jian, Han Wang, et al. Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study[J]. Materials Research Letters, 2021, 9(9): 373-381.
Xin Li Phuah, Jie Jian, Han Wang, 等. Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study[J]. 材料研究快报（英文）, 2021,9(9):373-381. DOI： 10.1080/21663831.2021.1927878.

Xin Li Phuah, Jie Jian, Han Wang, et al. Ultra-high heating rate effects on the sintering of ceramic nanoparticles: an in situ TEM study[J]. Materials Research Letters, 2021, 9(9): 373-381. DOI： 10.1080/21663831.2021.1927878.

摘要

Heating rate plays a major role in the ceramic sintering process

especially in many new advanced sintering techniques. In this study

the effects of ultra-high heating rate up to 1200°C/s have been investigated on

various ceramic nanoparticles by

in situ

transmission electron microscopy (TEM) heating experiments to monitor the morphological changes immediately after the heating process and during the holding time. It was revealed that an ultra-high heating rate is highly effective in densifying 3 mol.% yttria-stabilized zirconia nanoparticles but was less effective for 8 mol.% yttria-stabilized zirconia or zinc oxide due to the competing diffusion mechanisms.

Abstract

Heating rate plays a major role in the ceramic sintering process

especially in many new advanced sintering techniques. In this study

the effects of ultra-high heating rate up to 1200°C/s have been investigated on various ceramic nanoparticles by

in situ

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