1. 东北林业大学 工程技术学院,哈尔滨,150040
2. 先进焊接与连接国家重点实验室(哈尔滨工业大学),哈尔滨,150001
纸质出版:2021
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李春伟, 田修波, 姜雪松, 等. 高离化率电-磁场协同增强HiPIMS高速沉积特性[J]. 哈尔滨工业大学学报, 2021,53(2):84-92.
LI Chunwei, TIAN Xiubo, JIANG Xuesong, et al. High deposition characteristic of (E-MF) HiPIMS at high ionization rate[J]. 2021, 53(2): 84-92.
李春伟, 田修波, 姜雪松, 等. 高离化率电-磁场协同增强HiPIMS高速沉积特性[J]. 哈尔滨工业大学学报, 2021,53(2):84-92. DOI: 10.11918/202003040.
LI Chunwei, TIAN Xiubo, JIANG Xuesong, et al. High deposition characteristic of (E-MF) HiPIMS at high ionization rate[J]. 2021, 53(2): 84-92. DOI: 10.11918/202003040.
为了使高功率脉冲磁控溅射(HiPIMS)技术在保持高离化率的条件下实现HiPIMS高速沉积过程
采用电场与磁场双外场协同作用改善HiPIMS放电与沉积特性.研究了电-磁场协同增强HiPIMS((E-MF)HiPIMS)和常规HiPIMS制备钒膜时的基体离子电流密度、发射光谱、钒膜表面形貌及表面粗糙度、截面形貌及沉积速率等
并探讨了(E-MF)HiPIMS模式的放电机理.研究表明:与HiPIMS相比
钒靶(E-MF)HiPIMS放电时的平板工件基体离子电流密度峰值增加了6倍
铜靶(E-MF)HiPIMS放电时的筒状工件基体离子电流密度峰值增加了13倍.(E-MF)HiPIMS放电时的Ar0谱线、Ar+谱线、V0谱线和V+谱线强度均显著增强
氩和钒的粒子离化率增加.(E-MF)HiPIMS制备的钒膜由V(111)和V(211)组成.(E-MF)HiPIMS制备的钒膜表面更加光滑平整且表面粗糙度由15.0 nm减小为9.6 nm;钒膜生长结构更加致密且沉积速率增加了约30%
而筒状工件转动条件下(E-MF)HiPIMS制备的铜膜的沉积速率增加了约50%.(E-MF)HiPIMS是一种高离化率高沉积速率的新型放电模式
该方法可有效规避常规HiPIMS较低沉积速率的技术缺陷.
HJ1.1mm] Aiming to enable high power impulse magnetron sputtering (HiPIMS) technology to achieve high-speed deposition process while maintaining high ionization rate
the electric and magnetic fields synergistic effect was applied to improve the HiPIMS discharge and deposition characteristics. The substrate ion current density
optical emission spectrum
surface morphology and surface roughness
cross-section morphology
and deposition rate of vanadium films prepared by electro-magnetic fields synergistically enhancing HiPIMS ((E-MF) HiPIMS) were investigated
and the intrinsic physical mechanism of (E-MF) HiPIMS was analyzed. Results show that compared with HiPIMS
the peak of substrate ion current density of the plate workpiece in the discharge of vanadium target (E-MF) HiPIMS increased seven times
and the peak of substrate ion current density of the cylinder-like workpiece in the discharge of copper target (E-MF) HiPIMS increased 14 times. The intensity of Ar0 spectral lines
Ar+ spectral lines
V0 spectral lines
and V+ spectral lines of (E-MF) HiPIMS all enhanced significantly
and the ionization rate of Ar and V particles increased. The vanadium films prepared by (E-MF) HiPIMS consists of V (111) and V (211). The surface of the vanadium films prepared by (E-MF) HiPIMS was much smoother
and the surface roughness was reduced from 15.0 nm to 9.6 nm. The growing structure of the vanadium films was much denser
and the deposition rate was increased by about 30%. The deposition rate of copper films prepared by (E-MF) HiPIMS increased by about 50% under the cylinder-like workpiece rotation conditions. (E-MF) HiPIMS is a novel discharge mode with high ionization rate and high deposition rate
which can effectively avoid the technical defect of low deposition rate of conventional HiPIMS.
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