汕头大学 机构 工学院,广东,汕头,515063
[ "卢羿汛,硕士研究生," ]
[ "程西云,教授,硕士生导师,博士," ]
纸质出版:2026
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卢羿汛, 程西云, 张国建, 等. FDM型金属3D打印的石蜡黏结剂/316L不锈钢粉末成型坯的脱脂工艺[J]. 机械科学与技术, 2026,45(3):533-539.
卢羿汛, 程西云, 张国建, et al. Degreasing Process of Paraffin Binder/316L Stainless Steel Powder Forming Blank for FDM Metal 3D Printing[J]. Mechanical Science and Technology for Aerospace Engineering, 2026, 45(3): 533-539.
卢羿汛, 程西云, 张国建, 等. FDM型金属3D打印的石蜡黏结剂/316L不锈钢粉末成型坯的脱脂工艺[J]. 机械科学与技术, 2026,45(3):533-539. DOI: 10.13433/j.cnki.1003-8728.20240050.
卢羿汛, 程西云, 张国建, et al. Degreasing Process of Paraffin Binder/316L Stainless Steel Powder Forming Blank for FDM Metal 3D Printing[J]. Mechanical Science and Technology for Aerospace Engineering, 2026, 45(3): 533-539. DOI: 10.13433/j.cnki.1003-8728.20240050.
为了改善石蜡黏接剂在溶剂脱脂时产生的安全和用时长等问题,采用催化脱脂+热脱脂工艺对石蜡316L不锈钢粉末FDM(Fused deposition modeling)成型坯进行了脱脂处理。研究了脱脂温度、催化剂流量和脱脂时间等催化工艺参数对成型坯脱脂率的影响,研究了成型坯厚度与催化脱脂时间的关系;通过差示扫描量热-热重分析,制定了合理的热脱脂工艺。结果表明:脱脂温度为130 ℃、催化剂流量为0.04 g/min的工艺参数下催化脱脂4 h后,大部分成型坯脱脂率为70.0% ~ 75.0%,去除了93%以上的石蜡,催化脱脂时间比溶剂脱脂缩短了42%;成型坯厚度越大脱脂时间越长,成型坯厚度宜控制在6.5 mm以下;SEM结果显示脱脂后的成型坯形成大量连通间隙。经过了600 ℃保温60 min的热脱脂工艺后,成型坯的黏接剂已大部分去除,成型坯无变形崩塌。
In order to improve the safety and durability of paraffin adhesives in the solvent degreasing
the 316L stainless steel powder FDM(Fused deposition modeling) was degreased by using the catalytic degreasing and hot degreasing process. The influences of the catalytic process parameters such as degreasing temperature
catalyst flow rate and degreasing time on the degreasing rate of forming billet were studied. Through differential scanning calorimetry-thermogravimetric analysis
a reasonable thermal degreasing process was developed. The results show that at a degreasing temperature of 130 ℃
catalyst flow rate of 0.04 g/min and catalytic degreasing time of 4 h
the degreasing rate of the most formed billet is 70% - 75%
more than 93% paraffin is removed
and the catalytic degreasing time is reduced by 42% comparing with that in the solvent degreasing. The larger the thickness of the forming billet
the longer the degreasing time
and the thickness of the forming billet should be controlled below 6.5 mm. The SEM results showed that a large number of interconnecting gaps were formed after degreasing. At a thermal degreasing temperature of 600 ℃ and catalytic degreasing time of 60 min
the most of the adhesive has been removed and the forming blank has no deformation and collapse.
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